# Evaluation of shear bond strength of orthodontic ceramic and metal brackets with zirconia: effects of adhesive systems and storage conditions

**Authors:** Aya A. Salama, Karim A. Shehab, Alaa Mohamed Naguib

PMC · DOI: 10.1007/s00784-026-06783-1 · Clinical Oral Investigations · 2026-03-18

## TL;DR

This study compares how well metal and ceramic orthodontic brackets stick to zirconia under different bonding and storage conditions.

## Contribution

The study reveals that ceramic brackets and HEMA-containing adhesives provide stronger bonds to zirconia than metal brackets and HEMA-free systems.

## Key findings

- Ceramic brackets showed higher shear bond strength than metal brackets.
- HEMA-containing adhesive systems provided greater bond strength than HEMA-free systems.
- Water storage resulted in higher bond strength compared to thermocycling.

## Abstract

The current study assessed the shear bond strength of two orthodontic bracket materials to zirconia using two bonding approaches and two storage settings.

Two bonding strategies were selected to bond metal and ceramic brackets to zirconia samples. Before being tested for Shear Bond Strength [SBS], samples were either subjected to 5,000 thermocycles or kept in water for 24 h. Samples were divided into 8 Groups [n = 10] represented as Group 1: Ceramic Brackets + HEMA-Free Bonding System + Water Storage, Group 2: Ceramic Brackets + HEMA-Containing Bonding System + Water Storage, Group 3: Metal Brackets + HEMA-Free Bonding System + Water Storage, Group 4: Metal Brackets + HEMA-Containing Bonding System + Water Storage, Group 5: Ceramic Brackets + HEMA-Free Bonding System + Thermocycling, Group 6: Ceramic Brackets + HEMA-Containing Bonding System + Thermocycling, Group 7: Metal Brackets + HEMA-Free Bonding System + Thermocycling, Group 8: Metal Brackets + HEMA-Containing Bonding System + Thermocycling. Several independent groups were compared using the Kruskal-Wallis test, and two independent groups were assessed using the Mann-Whitney U test. A P-value < 0.05 was deemed significant.

Shear bond strength was significantly greater in ceramic than in metal [5.9 ± 2.6 vs. 4.9 ± 2.3, p = .026] and in 2-Hydroxyethyl methacrylate HEMA-containing systems compared to HEMA-free systems [6.1 ± 2.3 vs. 4.8 ± 2.4, p = .034]. Water storage settings also yielded higher bond strength than thermocycling conditions [6.9 ± 1.8 vs. 3.9 ± 2.2, p < .001].

The findings indicate that shear bond strength was significantly influenced by bracket material and adhesive system to zirconia. Additionally, storage settings play a crucial part in shear bond strength.

Developing effective bonding techniques for orthodontic brackets and zirconia ceramic materials remains a major clinical obstacle.

## Linked entities

- **Chemicals:** 2-Hydroxyethyl methacrylate (PubChem CID 13360), HEMA (PubChem CID 13360)

## Full-text entities

- **Diseases:** tooth injury (MESH:D018677), fracture (MESH:D050723)
- **Chemicals:** CQ (MESH:C048021), T (MESH:D014316), Yttria (MESH:C091417), C-HF-T (-), -HF (MESH:D006195), silane (MESH:D012821), Zirconia (MESH:C028541), Aluminum oxide (MESH:D000537), Transbond XT (MESH:C477790), Bis-EMA (MESH:C041979), 2-Hydroxyethyl methacrylate (MESH:C005044), camphorquinone (MESH:C553149), Bis-GMA (MESH:D017438), phosphate (MESH:D010710), Water (MESH:D014867), DMAEMA (MESH:C049840), TEGDMA (MESH:C020946), 10- methacryloyloxydecyl dihydrogen phosphate (MESH:C069749), SiC (MESH:C022088), Metal (MESH:D008670), Hafnium oxide (MESH:C545179)
- **Species:** Homo sapiens (human, species) [taxon 9606]

## Full text

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## Figures

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Source: https://tomesphere.com/paper/PMC12995977