# The mechanical and microstructural characteristics of low-energy calcined clay from a high-Egyptian gray clay with hydrated lime for rendering mortar applications

**Authors:** Karam S. Salama, Essam A. Kishar, Doaa A. Ahmed, Mohamed E. Saraya, Ezzat A. El-Fadaly, Aya Allah M. Ebrahim

PMC · DOI: 10.1038/s41598-026-37982-1 · Scientific Reports · 2026-02-27

## TL;DR

This study explores using low-energy calcined clay and hydrated lime to create eco-friendly mortars suitable for rendering applications, particularly in historic structure preservation.

## Contribution

The study introduces a cost-effective and environmentally friendly lime-clay binder for render mortars with optimized mechanical properties.

## Key findings

- The L40 mix (60% CCL and 40% HL) achieved compressive and flexural strengths of 13.2 MPa and 3.2 MPa, respectively.
- The R35Y render mortar (35% L40 and 2% Fe2O3) met EN998-1/2010 standards with strengths of 5.2 MPa and 2.1 MPa.
- The proposed mortars offer a sustainable solution for decorative and protective coatings in historic preservation.

## Abstract

The production of Portland cement has a significant global impact. Consequently, research into clinker replacement materials and alternative low-CO2 cements is becoming increasingly important to minimize their carbon footprint. For this study, limestone and raw clay were sourced from various locations in Egypt. These materials were calcined in a kiln at temperatures of 950 °C and 750 °C for 2 h, respectively. The primary goal of this study is to prepare and render mortars based on calcined clay with lime as a low-energy binder. The research primarily focuses on the mechanical and microstructural properties of lime-clay mortars and lime-clay render mortars, specifically hydrated lime (HL) and calcined clay (CCL). The mechanical and physical properties of these mortars were tested according to EN 196-1, using a mixing ratio of 1:3 (binder to sand) with total weight proportions of 450:1350. Water was added to achieve the necessary consistency and workability for this type of mortar, with an amount of approximately 302 ± 5 g. The results suggest that the most recommended proportion for optimal mortar performance with the used binder (CCL-HL) is L40, mainly consisting of 60% CCL and 40% HL with a water-to-solid ratio of approximately 0.17. The compressive and flexural strengths for the CCL-HL mortar sample (L40) are 13.2 MPa and 3.2 MPa, respectively. Additionally, the preparation of render mortars using this binder (L40) demonstrates that the most cost-effective and environmentally friendly binder proportion is R35Y, which consists of 35% L40 and 2% Fe2O3 as a yellow pigment, with a water-to-solid ratio of approximately 0.30. The compressive and flexural strengths of the R35Y render mortar are 5.2 and 2.1 MPa, respectively. The findings demonstrate that all prepared CCL-HL render mortars are suitable for rendering applications, meeting the requirements of EN998-1/2010 and offering a cost-effective, environmentally conscious solution for decorative and protective coatings, particularly in the preservation of historic structures.

## Linked entities

- **Chemicals:** Fe2O3 (PubChem CID 14833)

## Full-text entities

- **Diseases:** CH (MESH:D002128)
- **Chemicals:** polymer (MESH:D011108), calcium silicate (MESH:C031293), C (MESH:D002244), HPMC (MESH:D065347), silicate (MESH:D017640), carbonate (MESH:D002254), CC (MESH:D002119), kaolinite (MESH:D007616), O (MESH:D010100), sulfate (MESH:D013431), magnetite (MESH:D052203), Fe2O3 (MESH:C000499), chromium (III) oxide (MESH:C023600), Water (MESH:D014867), Al2O3 (MESH:D000537), CaF2 (MESH:D002124), CH (MESH:D002126), epoxy resin (MESH:D004853), ettringite (MESH:C501337), Al (MESH:D000535), CCL (-), PG (MESH:C077769), Si (MESH:D012825), aluminosilicate (MESH:C049037), Calcium aluminate (MESH:C035219), SiO2 (MESH:D012822), H+ (MESH:D006859), chromium oxide (MESH:C053245), LH (MESH:D007986), oxides (MESH:D010087), CA (MESH:D002118), Lime (MESH:C016538), quartz (MESH:D011791), CO2 (MESH:D002245), OH (MESH:C031356)
- **Species:** Sus scrofa (pig, species) [taxon 9823], Hyphomicrobium sp. PMC (species) [taxon 161967]
- **Mutations:** R25G, 25  C, R25, R30Y, L30, R35Y, stop for 15, R25Y, R33Y, R30G, R35Y, R35G

## Full text

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## Figures

16 figures with captions in the complete paper: https://tomesphere.com/paper/PMC12954124/full.md

## References

8 references — full list in the complete paper: https://tomesphere.com/paper/PMC12954124/full.md

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Source: https://tomesphere.com/paper/PMC12954124