# Texture Evolution and In Situ Investigation of Recrystallization Behavior in a Hot-Rolled Al-Zn-Mg-Cu-Zr Alloy

**Authors:** Peng Xia, Kedu Lin, Yiwen Hu, Jianfei Hao, Runxia Li, Huilan Huang

PMC · DOI: 10.3390/ma19040665 · 2026-02-09

## TL;DR

This study examines how different homogenization treatments affect the texture and recrystallization behavior in a specific aluminum alloy during hot rolling.

## Contribution

The novel contribution is the in situ investigation of how Al3Zr precipitates modulate recrystallization behavior in hot-rolled Al-Zn-Mg-Cu-Zr alloys.

## Key findings

- Double-stage homogenized alloy showed suppressed recrystallization due to higher Al3Zr precipitate density.
- Single-stage homogenized alloy exhibited extensive recrystallization peaking at 78.1%.
- Brass-oriented grains transformed into cube-oriented grains during recrystallization.

## Abstract

By means of characterization techniques such as XRD, TEM, and in situ EBSD, the texture evolution, recrystallization behavior, and their modulation by the Al3Zr phase in hot-rolled Al-Zn-Mg-Cu-Zr alloys with varied homogenization treatments were investigated. Results show that both the single-stage homogenized (SH) alloy and the double-stage homogenized (DH) alloy acquired a typical β-fiber texture after hot rolling, including brass, S, and copper orientations. The DH alloy experienced suppressed recrystallization (a recrystallization fraction of 6.05%) owing to its higher density of Al3Zr precipitates. In contrast, the SH alloy exhibited more significant dissolution and agglomeration of Al3Zr, leading to extensive recrystallization peaking at 78.1%. The primary recrystallization mode was identified as continuous recrystallization, characterized by the growth and coarsening of subgrains. Although dynamically recrystallized (DRx) grains formed during hot rolling could act as potential recrystallization nuclei, most of them exhibited weak growth capability, except the cube-oriented grains. During recrystallization, deformed grains with S orientation tended to transform into cube-oriented grains, while those with brass orientation prefer to convert into Goss-oriented grains. This can be attributed to the presence of highly mobile grain boundaries between these specific orientation pairs. In the DH alloy, subgrain growth and DRx grain consumption during annealing reduced orientation dispersion in deformed grains, promoting marked brass texture strengthening, with its volume fraction reaching 57.7%.

## Full-text entities

- **Genes:** RBPJ (recombination signal binding protein for immunoglobulin kappa J region) [NCBI Gene 3516] {aka AOS3, CBF-1, CBF1, IGKJRB, IGKJRB1, KBF2}
- **Diseases:** dislocation (MESH:D004204), injury to (MESH:D014947), EBSD (MESH:D028361)
- **Chemicals:** Mn (MESH:D008345), Mg (MESH:D008274), Al-Cu-Mg alloy (-), Al (MESH:D000535), Zr (MESH:D015040), S (MESH:D013455), Brass (MESH:C048399), alloy (MESH:D000497), Cu (MESH:D003300), Sc (MESH:D012538), P (MESH:D010758), Zn (MESH:D015032)
- **Species:** Homo sapiens (human, species) [taxon 9606]

## Figures

18 figures with captions in the complete paper: https://tomesphere.com/paper/PMC12941792/full.md

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Source: https://tomesphere.com/paper/PMC12941792