# The Effect of Thermocycling on the Microhardness of Contemporary Glass Ionomer-Based Restorative Materials: An In Vitro Study

**Authors:** Enes Bardakci, Didem Ozdemir Ozenen, Izzet Yavuz

PMC · DOI: 10.3390/bioengineering13020161 · Bioengineering · 2026-01-29

## TL;DR

This study compares how three dental restorative materials hold up under simulated oral aging, finding that one performs better than the others.

## Contribution

The study introduces a direct comparison of three modern glass ionomer materials' microhardness after thermocycling, relevant for pediatric dentistry.

## Key findings

- Thermocycling significantly reduced microhardness in all tested materials.
- Beautifil Bulk Restorative showed the highest microhardness before and after thermocycling.
- EQUIA Forte HT had the lowest microhardness, suggesting suitability for primary teeth.

## Abstract

Glass ionomer-based restorative materials are widely used in pediatric dentistry because of their chemical adhesion to tooth structure, ion-releasing capacity, and clinical handling advantages; however, their mechanical durability under simulated oral aging conditions remains a critical factor influencing long-term clinical performance. This in vitro study aimed to evaluate and compare the surface microhardness of three contemporary glass ionomer-based restorative materials—Beautifil Bulk Restorative, EQUIA Forte HT, and Fuji II LC—before and after thermocycling. A total of 90 disc-shaped specimens (10 mm in diameter and 2 mm in thickness) were prepared, with 30 samples allocated to each material group. Microhardness measurements were performed using the Vickers hardness test at baseline and after 10,000 thermocycling cycles between 5 °C and 55 °C to simulate intraoral aging. Results were expressed as the mean ± standard deviation, and statistical analyses were conducted using non-parametric tests. Thermocycling resulted in a statistically significant reduction in microhardness values for all tested materials (p < 0.05). Beautifil Bulk Restorative exhibited the highest microhardness values both before and after thermocycling, followed by Fuji II LC and EQUIA Forte HT, with significant differences observed among all groups (p < 0.001). Within the limitations of this study, Beautifil Bulk Restorative may be considered a favorable option for restorations in young permanent teeth, whereas EQUIA Forte HT, exhibiting lower microhardness values, may be more suitable for primary teeth, where physiological wear is expected.

## Full-text entities

- **Diseases:** injury to (MESH:D014947), Dental caries (MESH:D003731), Fuji II LC (MESH:C537730), chronic diseases (MESH:D002908)
- **Chemicals:** polymer (MESH:D011108), Glass Ionomer (MESH:C015897), Fuji II LC (MESH:C079765), water (MESH:D014867), fluoride (MESH:D005459), Beautifil (-)
- **Species:** Homo sapiens (human, species) [taxon 9606]
- **Cell lines:** Fuji — Homo sapiens (Human), Monophasic synovial sarcoma, Cancer cell line (CVCL_D880)

## Full text

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## Figures

2 figures with captions in the complete paper: https://tomesphere.com/paper/PMC12938537/full.md

## References

32 references — full list in the complete paper: https://tomesphere.com/paper/PMC12938537/full.md

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Source: https://tomesphere.com/paper/PMC12938537