# Strategic niobium integration and thermomechanical processing in the advancement of novel CMnSiAlPMo TRIP-aided bainitic steel

**Authors:** Hoda Refaiy, Eman El-Shenawy, Jukka Kömi, Mohammed Ali

PMC · DOI: 10.1038/s41598-026-38448-0 · Scientific Reports · 2026-02-24

## TL;DR

This paper explores how adding niobium and using different processing methods affects the properties of a new type of bainitic steel.

## Contribution

The study introduces a novel CMnSiAlPMo TRIP-aided bainitic steel with strategic niobium integration and evaluates its processing effects.

## Key findings

- Increasing deformation passes and lowering final deformation temperature improved flow behavior and hardness in the steel alloys.
- Niobium addition refined microstructure and increased peak flow stress in the four-pass processing regime.
- Grain refinement was more influential than retained austenite fraction in determining hardness outcomes.

## Abstract

This study examines the effects of niobium (Nb) addition and different thermomechanical controlled processing (TMCP) regimes on the flow stress behaviour and microstructure evolution of a newly developed CMnSiAlPMo TRIP-aided bainitic steel. TMCP tests were conducted with various hot deformation passes, followed by austempering at 400 °C for 10 min using a Gleeble 3800 thermomechanical simulator. Microstructures were analysed using scanning electron microscopy with electron backscattering diffraction and X-ray diffraction. Results showed that increasing the number of passes and reducing the final deformation temperature (FDT) enhanced the flow behaviour for both 0Nb and 0.05Nb alloys, with strain hardening being the dominant mechanism across all regimes. The four-pass regime with an FDT of 850 °C for the 0Nb alloy achieved the highest hardness (457 HV), attributed to grain refinement, which was more influential than the retained austenite fraction. For the 0.05Nb alloy, the two-pass regime at 1050 °C showed the highest hardness (428 HV), resulting from a lower retained austenite fraction. Additionally, Nb addition significantly refined the microstructure and increased the peak flow stress from 385 MPa to 421 MPa for the four-pass regime. The prior austenite grain size decreased from 23 to 12 μm in the single-pass regime, and the largest grain size in the cumulative grain size distribution (D90%) decreased from 8.45 to 7.49 μm.

## Linked entities

- **Chemicals:** niobium (PubChem CID 23936)

## Full-text entities

- **Genes:** ATM (ATM serine/threonine kinase) [NCBI Gene 472] {aka AT1, ATA, ATC, ATD, ATDC, ATE}
- **Diseases:** TMCP (MESH:D007174), Dislocation (MESH:D004204), TBS (MESH:D010411)
- **Chemicals:** silica (MESH:D012822), Al (MESH:D000535), Si (MESH:D012825), C-Mn-Si-Al-P-Mo TRIP (-), NbC (MESH:D009675), Mn (MESH:D008345), Mo (MESH:D008982), Phosphorus (MESH:D010758), steel (MESH:D013232), ferrite (MESH:C001215), polymer (MESH:D011108), C (MESH:D002244), Ni (MESH:D009532), N (MESH:D009584), Fe (MESH:D007501), Nb (MESH:D009556), Cu (MESH:D003300), AlN (MESH:C052045)

## Full text

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## Figures

15 figures with captions in the complete paper: https://tomesphere.com/paper/PMC12932859/full.md

## References

17 references — full list in the complete paper: https://tomesphere.com/paper/PMC12932859/full.md

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Source: https://tomesphere.com/paper/PMC12932859