# Characterization of key volatile compounds in meat-based broths using HS-SPME-Arrow-GC/MS and their relationship to sensory perception

**Authors:** Jin-Kyung Nam, Mi-Ran Kim, Jeong Eun Hyeon, Hae Won Jang

PMC · DOI: 10.1016/j.fochx.2026.103601 · Food Chemistry: X · 2026-01-27

## TL;DR

This study identifies key volatile compounds in meat-based broths and links them to sensory qualities like meaty aroma and umami taste.

## Contribution

The first systematic volatile profiling of commercial meat-based broths is reported.

## Key findings

- Eighteen volatile compounds were identified, with aldehydes being the most abundant.
- Key aldehydes like decanal, heptanal, and hexanal contribute fatty notes and correlate with consumer liking.
- Pyrazines and methional were found only in beef flavoring ingredients, not in broths.

## Abstract

Meat-based broths are increasingly popular with consumers; however, their volatile profiles remain underexplored. This study uses headspace solid-phase microextraction-Arrow combined with gas chromatography/mass spectrometry to identify and quantify volatile compounds in commercial meat-based broths. The analytical method was optimized using response surface methodology and validated through calibration curves, limits of detection and quantification, and recovery analyses to ensure sensitivity and accuracy. Eighteen volatile compounds were identified, with aldehydes being the most abundant. Several compounds, including aldehydes contributing fatty characteristics, were identified in meat-based broths as well as beef flavoring ingredients (extract and powder), whereas pyrazines and methional were found only in beef flavoring ingredients. In sensory evaluations, samples with strong meaty odors and rich umami tastes received high ratings, whereas weak odors and flavors or low saltiness yielded poor consumer acceptance. By identifying key volatile compounds in meat-based broths, this study provides insight for developing Korean-style home meal replacement products.

Unlabelled Image

•The first systematic volatile profiling of commercial meat-based broths is reported.•Integrated chemical and sensory analyses reveal key flavor contributors.•Key aldehydes (decanal, heptanal, hexanal, nonanal, and octanal) impart fatty notes.•Strong correlations are observed between key aldehydes and consumer liking.

The first systematic volatile profiling of commercial meat-based broths is reported.

Integrated chemical and sensory analyses reveal key flavor contributors.

Key aldehydes (decanal, heptanal, hexanal, nonanal, and octanal) impart fatty notes.

Strong correlations are observed between key aldehydes and consumer liking.

## Linked entities

- **Chemicals:** decanal (PubChem CID 8175), heptanal (PubChem CID 8130), hexanal (PubChem CID 6184), nonanal (PubChem CID 31289), octanal (PubChem CID 454), pyrazines (PubChem CID 9261), methional (PubChem CID 18635)

## Full-text entities

- **Chemicals:** HS (MESH:D006859), aldehydes (MESH:D000447), methional (MESH:C008390), pyrazines (MESH:D011719), fatty (-), SPME (MESH:C056082)

## Full text

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## Figures

4 figures with captions in the complete paper: https://tomesphere.com/paper/PMC12887422/full.md

## References

40 references — full list in the complete paper: https://tomesphere.com/paper/PMC12887422/full.md

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Source: https://tomesphere.com/paper/PMC12887422