# Effect of immersion in different media on the color stability, surface roughness, and microhardness of flowable nanohybrid resin composites

**Authors:** Hend Yousri Abd-Elfattah, Mohamed Elshirbeny Elawsya, Abeer ElSayed ElEmbaby

PMC · DOI: 10.1186/s12903-025-07555-1 · BMC Oral Health · 2026-01-12

## TL;DR

This study tested how different liquids affect the color, roughness, and hardness of dental resin composites.

## Contribution

The study provides new empirical data on how various immersion media impact flowable nanohybrid resin composites.

## Key findings

- Energy drinks caused the most significant discoloration and increased roughness in tested resin composites.
- All tested media reduced microhardness of the resin composites compared to the control.
- Polofil NHT Flow showed the highest increase in surface roughness after immersion in energy drinks.

## Abstract

To evaluate color stability, surface roughness, and microhardness of flowable nanohybrid resin composites following immersion in different media.

Polofil NHT Flow (VOCO GmbH), G-aenial Universal Injectable (GC DENTAL PRODUCTS CORP), and Tetric N-Ceram (Ivoclar Vivadent) were used. From each tested resin composite, 50 disc-shaped specimens (10-mm diameter × 2-mm thickness) were performed. Each group was categorized into five subgroups according to immersion media (n = 10): (1) control (without immersion), (2) artificial saliva, (3) coffee, (4) cola, and (5) energy drink. Color stability, surface roughness, and microhardness were evaluated. Data were analyzed through two-way ANOVA, Tukey’s post-hoc, and Pearson correlation coefficient tests (p < 0.05).

For color change, no statistically significant differences were observed among the resin composites regarding artificial saliva (p = 0.78), coffee (p = 0.93), and cola (p = 0.09), while there was a significant difference between them regarding energy drink (p < 0.05). The highest surface roughness mean value was recorded with Polofil NHT Flow, which showed an increase in surface roughness after immersion in energy drink (0.32 ± 0.06 μm) compared to the control subgroup (0.22 ± 0.08 μm). For all resin composites, there were significant reductions in microhardness with all immersion media in comparison to the control subgroups (p < 0.05).

For color stability, energy drink and coffee had the most negative effect on all tested resin composites. Energy drink caused the highest discoloration with G-aenial Universal Injectable and the highest roughness with Polofil NHT Flow. All tested resin composites showed a decrease in surface microhardness following immersion in all tested immersion media.

## Full-text entities

- **Diseases:** gingival inflammation (MESH:D007249), teeth erosion (MESH:D018677), caries (MESH:D003731), discoloration (MESH:D014075), bacterial (MESH:D001424)
- **Chemicals:** INS 102 (MESH:D013645), Water (MESH:D014867), hydrogen (MESH:D006859), Bis GMA (MESH:D017438), silane (MESH:D012821), polymer (MESH:D011108), Bis-EMA (MESH:C041979), UDMA (MESH:C029824), Resin (MESH:D012116), oxygen (MESH:D010100), INS 110 (MESH:C005842), Bis (MESH:D001729), Bisphenol A ethoxylate dimethacrylate (-), citric acid (MESH:D019343), TEGDMA (MESH:C020946), riboflavin (MESH:D012256), phosphoric acid (MESH:C030242)
- **Species:** Homo sapiens (human, species) [taxon 9606]

## Full text

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## Figures

7 figures with captions in the complete paper: https://tomesphere.com/paper/PMC12879416/full.md

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Source: https://tomesphere.com/paper/PMC12879416