# Influence of reinforcement on the fracture surface characteristics of multistage solutionized and precipitation-hardened ternary Al-Mg-Si hybrid composites

**Authors:** Manjunath Shettar, Nitesh Kumar, Girish Hariharan, Gowri shankar, Ananda Hegde

PMC · DOI: 10.1038/s41598-025-34581-4 · Scientific Reports · 2026-01-03

## TL;DR

This study explores how adding SiC, B₄C, and their hybrid to an Al-Mg-Si alloy affects its fracture surface and mechanical properties after heat treatment.

## Contribution

The novelty lies in combining hybrid reinforcements with multistage solutionizing and aging to enhance strength and fracture resistance in Al 6061 composites.

## Key findings

- MSS-aged samples achieved a peak hardness of 222 VHN, a 177% improvement over as-cast samples.
- Hybrid composites showed a 124% increase in UTS, reaching 287 MPa.
- Hybrid composites displayed refined dimples and strong interfacial bonding, improving crack resistance.

## Abstract

This study investigates the effect of SiC, B₄C, and hybrid (SiC + B₄C) reinforcements on the fracture surface characteristics of multistage solutionized and precipitation-hardened Al-Mg-Si (Al 6061) alloy. Composites are fabricated using two-stage stir casting with SiC (1–3 wt%), B₄C (1–3 wt%), and hybrid reinforcements (1–2 wt% each). As-cast (AC) samples are subjected to single-stage solutionizing (SSS) and multistage solutionizing (MSS), followed by artificial aging at 100 and 200 °C. Results show that MSS-aged samples exhibit a peak hardness of 222 VHN, a 177% improvement over AC (80 VHN). Similarly, UTS increases from 128 MPa (AC) to 287 MPa in hybrid composites, marking a 124% enhancement. Fractography shows that unreinforced Al 6061 failed mainly in a ductile mode with coarse dimples, while monolithic composites exhibit mixed ductile–brittle features. Hybrid composites exhibit refined dimples and strong interfacial bonding, thereby enhancing crack resistance. AAHT-treated samples show a shift toward brittle-dominant failure. The combined effect of dual reinforcements and MSS treatment enhances both strength and fracture resistance, demonstrating the potential of Al 6061 hybrid composites for lightweight structural applications.

## Linked entities

- **Chemicals:** SiC (PubChem CID 9863)

## Full-text entities

- **Chemicals:** Si (MESH:D012825), Al (MESH:D000535), Mg (MESH:D008274)

## Full text

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## Figures

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## References

1 references — full list in the complete paper: https://tomesphere.com/paper/PMC12864847/full.md

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Source: https://tomesphere.com/paper/PMC12864847