# Experimental Study on the Effect of Humidity on the Mechanical Properties of 3D-Printed Mechanical Metamaterials

**Authors:** Qian Sun, Xiaojun Tan, Jianhao Man, Shuai Li, Zeeshan Ali, Kaiyang Yin, Bo Cao, Christoph Eberl

PMC · DOI: 10.3390/polym17212938 · 2025-11-03

## TL;DR

This study explores how humidity affects the mechanical properties of 3D-printed materials and metamaterials, showing significant changes in strength and behavior under different humidity levels.

## Contribution

The study systematically validates the impact of humidity on 3D-printed mechanical metamaterials, identifying critical thresholds for material behavior.

## Key findings

- Water absorption in polymers occurs in three stages with Nylon showing the highest uptake.
- Material properties like Poisson’s ratio shift abruptly at high humidity levels.
- Mechanical metamaterials exhibit predictable behavior at low-to-moderate humidity but become unpredictable at high humidity.

## Abstract

In this study, six common fused filament fabrication (FFF) polymers—PEEK, PLA, PETG, ABS, Nylon, and TPU—were acclimatized at 15%, 45%, and 95% relative humidity (RH) to characterize tensile behavior, including Young’s modulus, maximum strain, and ultimate tensile strength. Separately, mechanical metamaterial samples at relative densities (RD) of 25%, 35%, and 45% were tested in compression at the same RH levels to evaluate stiffness, strength, and Poisson’s ratio. The water absorption process can generally be divided into different stages—rapid uptake (0–12 h), a plateau (12–60 h), and a late rebound (60–100 h)—with a total uptake ranking of Nylon > PETG > PLA ≈ ABS > TPU ≈ PEEK. Samples under tensile and compressive tests show a great difference between properties at different RD and RH levels. Poisson’s ratio indicates that material responses remain predictable at low-to-moderate RH, whereas high RH serves as a critical threshold inducing abrupt Poisson’s ratio behavioral shifts. This study provides systematic validation for the application of 3D-printed metamaterials under varying humidity conditions, such as biomedical implants in human body.

## Full-text entities

- **Chemicals:** polymers (MESH:D011108), TPU (-), Nylon (MESH:D009757), PETG (MESH:C066907), water (MESH:D014867), PLA (MESH:C033616), PEEK (MESH:C063834)
- **Species:** Homo sapiens (human, species) [taxon 9606]

## Figures

12 figures with captions in the complete paper: https://tomesphere.com/paper/PMC12608748/full.md

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Source: https://tomesphere.com/paper/PMC12608748