# Influence of co-blending fly ash and ceramic waste powder on the performance and microstructure of cementitious substrates under sulfate dry-wet cycle attack

**Authors:** Xinyan Wang, Lu Zhang, Haizhou Li

PMC · DOI: 10.1371/journal.pone.0314277 · PLOS ONE · 2025-02-21

## TL;DR

This study explores how mixing fly ash and ceramic waste powder in cement improves its resistance to sulfate erosion under dry-wet cycles.

## Contribution

The novel contribution is identifying optimal SCM mix ratios and their impact on sulfate resistance in cementitious materials.

## Key findings

- Cement with fly ash and ceramic waste powder shows best sulfate resistance under dry-wet cycles.
- Water-to-binder ratio most affects corrosion resistance at 7 days.
- SCM content significantly impacts long-term corrosion resistance after 56 days.

## Abstract

This study examines the properties of cement-based materials incorporating composite additions of fly ash and ceramic waste powder (CWP) as supplementary cementitious materials (SCM). The resistance of the materials to sulfate erosion under dry-wet cycling conditions was investigated through experimental testing. A Box-Behnken Design was employed to establish a model using three factors: the replacement ratio of cement by SCMs, the mass ratio of CWP to SCMs, and the water-to-binder ratio. The response variable was the mass loss rate due to sulfate erosion after 24 cycles of dry-wet cycling. Significance analysis of single-factor and multiple-factor interactions was conducted based on the response surface model. The research findings indicate that the cement-based materials with combined additions of fly ash and CWP exhibit optimal resistance to sulfate erosion under dry-wet cycling conditions. The water-to-binder ratio was identified as the most significant factor affecting the corrosion resistance of the cement-based materials at 7 days of curing. The dosage of ceramic waste powder influenced the corrosion performance of the cement-based materials at 28 days of curing. The content of SCMs affected the corrosion resistance of the cement-based materials after 56 days of curing. Comparative analysis of the grayscale three-dimensional distribution map and histogram of the cement-based materials with SCMs revealed an increase in the compactness of the matrix.

## Full text

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## Figures

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## References

49 references — full list in the complete paper: https://tomesphere.com/paper/PMC11845027/full.md

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Source: https://tomesphere.com/paper/PMC11845027