# Deep Indentation Tests of Soft Materials Using Mobile and Stationary Devices

**Authors:** Joanna Nowak, Mariusz K. Kaczmarek

PMC · DOI: 10.3390/ma17174233 · Materials · 2024-08-27

## TL;DR

This study compares indentation testing of soft materials using mobile and stationary devices, showing that deep indentation can effectively characterize material properties.

## Contribution

The study introduces a deep indentation method that effectively captures elastic properties of soft materials and their layered structures.

## Key findings

- Maximum forces during indentation and slopes of force curves effectively characterize foam materials and silicone layers.
- Deep indentation distinguishes itself from shallow methods by capturing properties of two-layer materials.
- Repeatability of tests is comparable between mobile and stationary devices.

## Abstract

Measurements of the properties of soft materials are important from the point of view of medical diagnostics of soft tissues as well as testing the quality of food products and many technical materials. One of the frequently used techniques for testing such materials, attractive due to its non-invasive nature, is the indentation technique, which does not puncture the material. The difficulty of testing soft materials, which affects the objectivity of the results, is related to the problems of stable positioning of the studied material in relation to the indentation apparatus, especially with a device held by the operator. This work concerns the comparison of test results using an indentation apparatus mounted on mobile and stationary handles. The tested materials are cylindrical samples of polyurethane foams with three different stiffnesses and the same samples with a 0.5 or 1 mm thick silicone layer. The study presented uses an apparatus with a flat cylindrical indenter, with a surface area of 1 cm2, pressed to a depth of 10 mm (so-called deep tests). Based on the recorded force changes over time, five descriptors of the indentation test were determined and compared for both types of handles. The tests performed showed that the elastic properties of foam materials alone and with a silicone layer can be effectively characterized by the maximum forces during recessing and retraction and the slopes of the recessing and retraction curves. In the case of two-layer materials, these descriptors reflect both the characteristics of the foams and the silicone layer. The results show that the above property of the deep indentation method distinguishes it from the shallow indentation method. The repeatability of the tests performed in the mobile and stationary holders were determined to be comparable.

## Full-text entities

- **Chemicals:** silicone (MESH:D012828), polyurethane (MESH:D011140)

## Full text

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## Figures

12 figures with captions in the complete paper: https://tomesphere.com/paper/PMC11395885/full.md

## References

52 references — full list in the complete paper: https://tomesphere.com/paper/PMC11395885/full.md

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Source: https://tomesphere.com/paper/PMC11395885