# Open-Source Data Analysis Tool for Spectral Small-Angle X-ray Scattering Using Spectroscopic Photon-Counting Detector

**Authors:** Sabri Amer, Andrew Xu, Aldo Badano, Eshan Dahal

PMC · DOI: 10.3390/s24165307 · Sensors (Basel, Switzerland) · 2024-08-16

## TL;DR

This paper introduces an open-source tool for analyzing sSAXS data using a 2D photon-counting detector, enabling detailed material characterization.

## Contribution

The novel contribution is an open-source graphical tool for sSAXS data analysis with energy-resolved capabilities.

## Key findings

- The tool successfully outputs 1D scattering patterns and 2D spatially-resolved maps.
- Validation with caffeine powder confirmed the tool's accuracy in capturing known scattering peaks.

## Abstract

Spectral small-angle X-ray scattering (sSAXS) is a powerful technique for material characterization from thicker samples by capturing elastic X-ray scattering data in angle- and energy-dispersive modes at small angles. This approach is enabled by the use of a 2D spectroscopic photon-counting detector that provides energy and position information of scattered photons when a sample is irradiated by a polychromatic X-ray beam. Here, we describe an open-source tool with a graphical interface for analyzing sSAXS data obtained from a 2D spectroscopic photon-counting detector with a large number of energy bins. The tool takes system geometry parameters and raw detector data to output 1D scattering patterns and a 2D spatially-resolved scattering map in the energy range of interest. We validated these features using data from samples of caffeine powder with well-known scattering peaks. This open-source tool will facilitate sSAXS data analysis for various material characterization applications.

## Linked entities

- **Chemicals:** caffeine (PubChem CID 2519)

## Full-text entities

- **Chemicals:** caffeine (MESH:D002110)

## Full text

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## Figures

6 figures with captions in the complete paper: https://tomesphere.com/paper/PMC11360091/full.md

## References

19 references — full list in the complete paper: https://tomesphere.com/paper/PMC11360091/full.md

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Source: https://tomesphere.com/paper/PMC11360091