Comprehensive determination of Burgers vectors of threading dislocations in GaN substrates by combining reflection and transmission synchrotron-radiation x-ray topography

TL;DR

This study presents a comprehensive method using combined reflection and transmission synchrotron-radiation x-ray topography to accurately determine Burgers vectors of threading dislocations in GaN substrates.

Contribution

It introduces a practical approach for complete Burgers vector determination by integrating reflection and transmission SR-XRT techniques.

Findings

Successfully identified Burgers vectors of individual threading dislocations.

Observed pairs of screw-type dislocations with opposite Burgers vectors.

Demonstrated the effectiveness of combined SR-XRT modes for dislocation analysis.

Abstract

Burgers vectors (b) of threading dislocations (TDs) in an acidic ammonothermal-grown GaN substrate were investigated using synchrotron radiation x-ray topography (SR-XRT) by combining both reflection and transmission modes. Reflection XRT images recorded with six equivalent g vectors of 11-24 revealed spot-like contrasts corresponding to TDs. Based on the contrast conditions, the possible Burgers vectors were constrained, and the c-axis component of b for mixed-type TDs was estimated from the contrast size. Using transmission XRT images recorded under several two-beam diffraction conditions, the (0001) in-plane direction of b was evaluated based on the gb invisibility criterion. Furthermore, by analyzing the linewidths of dislocation images observed under kinematical diffraction contrast, the magnitude of the a-axis component of b was determined. By combining these analyses, the Burgers vectors of individual TDs, including edge- and mixed-type dislocations, were determined. In addition, a pair of screw-type TDs with opposite Burgers vectors, +1c, -1c, was observed in the transmission SR-XRT. These results demonstrate that the combined use of reflection and transmission SR-XRT provides a practical approach for complete determination of Burgers vectors in GaN substrates.