The effects of high-temperature ion-irradiation on early-stage grain boundaries serrations formation in Ni-based alloys

TL;DR

This study investigates how high-temperature ion irradiation affects grain boundary serrations in Ni-based alloys, revealing hardening effects and morphological changes, with implications for nuclear reactor materials.

Contribution

It provides new insights into radiation-induced microstructural changes and deformation mechanisms in Hastelloy X and Haynes 230 alloys under ion irradiation.

Findings

Radiation causes hardening in both alloys.

Hastelloy X shows more pronounced effects.

Significant precipitate morphology changes in Hastelloy X.

Abstract

Nickel based superalloys display outstanding properties such as excellent creep strength, remarkable fracture toughness parameters, and corrosion resistance. For this reason, Ni based materials are considered as materials dedicated to the IV generation of nuclear reactors. Although these materials seem promising candidates, their radiation resistance and impact of radiation damage on the deformation mechanism are still not fully understood. In this work, two commercially available nickel based alloys, Hastelloy X and Haynes 230, were investigated. Structural and mechanical properties have been described by means of SEM and EBSD, TEM, and nanoindentation tests. Radiation damage has been performed by Ar ion with energy 320keV with two doses up to 12dpa. Obtained results have revealed a hardening effect for both levels of damage. However, more intensive effects were observed for Hastelloy X. Moreover, a significant change in precipitates morphology in Hastelloy X has been observed. It has been proposed that structural differences between both alloys determine the type of occurring radiation induced processes. Excess energy deposited into materials structure during ion irradiation can lower the temperature of nucleation of high temperature phases, which initiates the formation of grain boundary serrations.