Investigation of quasi-cleavage in a hydrogen charged maraging stainless steel

TL;DR

This study investigates how hydrogen influences quasi-cleavage cracking in PH13-8Mo maraging stainless steel, revealing a discontinuous crack propagation mechanism involving brittle cracks and ductile ridges.

Contribution

It provides detailed fractographic and EBSD analysis of hydrogen-assisted quasi-cleavage, highlighting a novel re-initiation mechanism of cracks.

Findings

Hydrogen accelerates quasi-cleavage crack growth.

Cracks propagate along {100} planes and are halted at high-angle boundaries.

Cracks are connected by ductile ridges, indicating a mixed brittle-ductile failure mode.

Abstract

Slow strain rates tests (SSRT) were conducted on hydrogen-containing specimens of PH13-8Mo maraging stainless steel. Hydrogen-assisted subcritical quasi-cleavage cracking was shown to take place during SSRT, thus accelerating material failure. Fractographic analysis showed that quasi-cleavage is composed of flat brittle areas and rougher areas. Using cross-sectional electron backscatter diffraction (EBSD) analysis of a secondary subcritically grown crack, we observed brittle cracks propagated across martensite blocks ahead the main crack tip. These cracks were stopped at high-angle boundaries. The crack direction was consistent with propagation along {100} type planes. High-resolution EBSD showed significant crystal lattice rotation, hence consequential plastic deformation, concentrated between the main crack tip and the cracks located ahead it. It is concluded that quasi-cleavage in the material investigated here consists of {100} cleavage cracks connected by ductile ridges. A discontinuous mechanism, involving re-initiation of new cleavage cracks ahead the main crack tip is suggested.