Effect of severe thermo-oxidative aging on the mechanical behavior and fatigue durability of short glass fiber reinforced PA6/6.6

TL;DR

This study investigates how severe thermo-oxidative aging affects the mechanical and fatigue properties of short glass fiber reinforced PA6/6.6, revealing aging impacts on fatigue life and the effectiveness of existing fatigue criteria.

Contribution

It provides new insights into the fatigue behavior of aged SFRP composites and evaluates the applicability of fatigue criteria developed for unaged materials to aged ones.

Findings

Aging increases stiffness and embrittlement, especially in V35 material.

Fatigue life is more affected in V35 than V50 after aging.

Cyclic creep energy-based criteria remain effective for aged composites.

Abstract

The work deals with the fatigue lifetime estimation of Short Fiber Reinforced Thermoplastics (SFRP), with a focus on conjugated effects of thermal aging. Two materials containing 35% (V35) and 50% (V50) weight ratio of short glass fibers were aged for 500h at 200{\textdegree}C in air and compared to the same materials in a Dry-As-Molded (DAM) state. Monotonic and fatigue tests were performed in samples machined out of injected plates and cut along three different orientations to the injection one (0, 45, 90{\textdegree}) in order to capture the anisotropy of the skin-core microstructure, classical in injected SFRP. Monotonic tensile tests evidenced the stiffening and embrittlement of the Polyamide matrix reported in the literature, nevertheless with an acuity depending on the matrix ratio and fiber orientation. Stress-controlled fatigue tests were performed at constant amplitude, frequency (10Hz), temperature (200{\textdegree}C) and stress ratio R=0.1. The fatigue curves of V35 are more affected by aging than those of the V50 material. The combined results from the mean strain evolutions and SEM observations confirmed that the initiation approach for fatigue lifetime estimation was still valid in aged composites. Several fatigue criteria, among the most recently reported in the literature, were evaluated from this database. The effect of aging on the cyclic evolution of the different Fatigue Indicator Parameters (FIP) involved in the criteria was analyzed preliminarily. For the present fatigue conditions, the best criteria for unaged materials (i.e cyclic creep energy-based ones) were shown to still be the best for aged materials. Finally, the ability to predict fatigue lifetime for aged composites from the identification of the fatigue criterion in the unaged state was evaluated.