Statistical analysis of dislocation cells in uniaxially deformed copper single crystals

TL;DR

This study uses HR-EBSD, X-ray analysis, and TEM to investigate dislocation microstructures in deformed copper single crystals, revealing internal stress, dislocation density, and fractal characteristics of dislocation cells.

Contribution

It introduces a comprehensive approach combining HR-EBSD, X-ray, and TEM to analyze dislocation structures and their evolution in copper crystals during deformation.

Findings

Internal stress observed in cell interiors

Fractal dimension decreases with dislocation density

Dislocation evolution monitored via SEM-based technique

Abstract

The dislocation microstructure developing during plastic deformation strongly influences the stress-strain properties of crystalline materials. The novel method of high resolution electron backscatter diffraction (HR-EBSD) offers a new perspective to study dislocation patterning. In this work copper single crystals deformed in uniaxial compression were investigated by HR-EBSD, X-ray line profile analysis, and transmission electron microscopy (TEM). With these methods the maps of the internal stress, the Nye tensor, and the geometrically necessary dislocation (GND) density were determined at different load levels. In agreement with the composite model long-range internal stress was directly observed in the cell interiors. Moreover, it is found from the fractal analysis of the GND maps that the fractal dimension of the cell structure is decreasing with increasing average spatial dislocation density fluctuation. It is shown that the evolution of different types of dislocations can be successfully monitored with this scanning electron microscopy based technique.