Computational Rheometry of Yielding and Viscoplastic Flow in Vane-and-Cup Rheometer Fixtures

TL;DR

This study uses computational simulations to analyze how vane-in-cup rheometer geometries affect the measurement accuracy of viscoplastic fluids, revealing the influence of vane structure, slip conditions, and Bingham number on flow fields and torque readings.

Contribution

It introduces a detailed two-dimensional computational approach to evaluate the effects of vane geometry and slip conditions on rheometric measurements of yield-stress fluids.

Findings

Fractal vanes with many arms improve measurement accuracy by cloaking internal structural features.

Slip on the vane surface does not significantly affect torque measurements.

Outer wall slip conditions significantly impact rheometric data.

Abstract

A planar two-dimensional computational analysis is presented to qualify traditional and fractal vane-in-cup geometries for accurate rheometry of simple viscoplastic fluids with and without slip. Numerical simulations based on an adaptive augmented Lagrangian scheme are used to study the two-dimensional flow field of yield-stress fluids within and around vane tools with N=3 to 24 arms for a wide range of Bingham numbers, B (i.e. the ratio of the yield stress over the characteristic viscous stress). This allows for accurate calculations of the velocity and stress fields around vanes with various geometries, as well as direct comparison to experimental observations of the output torque measured by a rheometer, revealing sources of variation and error. We describe the impact of the vane structure on the fluid velocity field, from few-arm cruciform vanes (N < 6) that significantly perturb the flow away from ideal azimuthal kinematics, to many-arm fractal vanes (N > 12) in which the internal structural features are successfully ``cloaked" by a yield surface. This results in the shearing of an almost-circular ring of viscoplastic fluid that is indistinguishable from the annular ring of fluid deformed around a slip-free rotating cylindrical bob and leads to more accurate rheometric measurements of the material flow curve. Moreover, in direct comparison with data from previous literature, we show that slip conditions on the vane surface do not impact the velocity field or measured overall torque T, whereas slip conditions on the smooth outer wall have significant impact on data, even when using a vane geometry. Finally, we describe the impact of vane topography and Bingham number, B, on the measured torque and rheometric accuracy of vane-in-cup geometries for ``simple" (inelastic) yield-stress fluids described by either the Bingham plastic or Herschel-Bulkley constitutive model.