Effect of Surface Roughness on Early Stage Oxidation Behavior of Ni-Base Superalloy IN 625

TL;DR

This study investigates how surface roughness affects the early oxidation behavior of Ni-base superalloy IN 625, revealing that surface preparation influences oxidation rate, oxide composition, and morphology during high-temperature exposure.

Contribution

It introduces a novel fractal analysis method for surface roughness and demonstrates its impact on oxidation behavior of IN 625, providing new insights into surface preparation effects.

Findings

Grinding reduces oxidation kinetics of IN 625

Surface roughness affects oxide scale composition and morphology

Different surface preparations lead to significant changes in oxidation behavior

Abstract

In the present work the effect of surface roughness on oxidation behavior during the early stages of high temperature exposure of Ni-base superalloy IN 625 is described. The surface roughness was described using standard contact profilometer as well as novel method, fractal analysis. It was found that the different surface preparation resulted in a difference in roughness with a parameter increase of at least one order of magnitude for the ground sample as compared with the polished sample. The oxidation test was performed in a horizontal tube furnace. Post exposure analyses including glow discharge optical emission spectrometry (GD OES) and scanning electron microscopy (SEM), which revealed that grinding lowers the oxidation kinetics of IN 625. It was found that surface preparation influences the oxide scale composition and morphology. The hypothesis explaining the mechanism responsible for the changes in oxidation behavior is proposed as well.