Strain heterogeneity and micro-damage nucleation under tensile stresses in an Mg-5Al-3Ca alloy with an intermetallic skeleton

TL;DR

This study investigates how strain heterogeneity and micro-damage nucleation occur at the microstructural level in an Mg-5Al-3Ca alloy during tensile deformation at elevated temperature, revealing the critical role of intermetallic phases in crack initiation and growth.

Contribution

It provides new insights into micro-scale strain localization, phase interactions, and crack nucleation mechanisms in Mg alloys with intermetallic skeletons under tensile stress.

Findings

Strain is mainly carried by the α-Mg phase.

Cracks nucleate in the Laves phase at specific microstructural features.

Cracks grow along Laves phases leading to fracture.

Abstract

Strain heterogeneity at the microstructural level plays a vital role in the deformation and fracture behaviour of dual or multi-phase materials. In the present work, the strain heterogeneity, localization and partitioning arising at the sub-micron scale during elevated temperature (170 {\deg}C) tensile deformation of an Mg-5Al-3Ca alloy was investigated using quasi in-situ {\mu}-DIC experiments. The results reveal that the strain is mainly carried by the {\alpha}-Mg phase, while the intermetallic Laves phase plays a critical role in that strain concentrations build up at the {\alpha}-Mg matrix and Laves phase interfaces, hence, reducing the overall deformability of the alloy. In quasi in-situ and bulk material analysis at elevated temperature, cracks were observed to nucleate in the Laves phase, at i) the intersection points of slip lines in the {\alpha}-Mg matrix with the Laves phase and ii) the twin intersections with {\alpha}-Mg/Laves phase interfaces and iii) twin transmissions across {\alpha}-Mg/Laves phase interfaces. Euler number analysis has shown that the (inter-)connectivity of the Laves phase decreases with deformation. Finally, cracks grow preferentially along the Laves phases until the material fractures.