# Shape anisotropy of magnetic nanoparticles in (Co$_{86}$Nb$_{12}$Ta$_2$)$_x$(SiO$_2$)$_{1-x}$ composite films revealed by grazing-incidence small-angle X-ray scattering

## TL;DR

This study investigates the shape anisotropy of magnetic nanoparticles in amorphous composite films using grazing-incidence small-angle X-ray scattering, revealing how nanoparticle size and shape evolve with metal concentration.

## Contribution

It provides new insights into the anisotropic growth and size variation of magnetic nanoparticles in composite films near the percolation threshold.

## Key findings

- Nanoparticle size increases with metal concentration.
- Particles are elongated perpendicular to the film plane.
- Shape anisotropy becomes more pronounced at higher concentrations.

## Abstract

Structure of amorphous nangranular composite (Co$_{86}$Nb$_{12}$Ta$_2$)$_x$(SiO$_2$)$_{1-x}$ films was studied by means of grazing-incidence small-angle X-ray scattering as a function of atomic concentration $x$ of the metal fraction in vicinity of the percolation threshold. It has been established that the average size of magnetic nanoparticles increases with $x$ and this increment exhibit the anisotropic character. It was found that in a whole concentration range the particles are elongated along the growth direction perpendicular to the film plane. For the lowest concentration $x=0.193$ clusters with isotropic shape and average radius of 1 nm were observed, while for higher concentrations up to $x=0.665$ the average cluster length along the film normal is $1.5-7$ nm and the cross-section is $1-2$ nm.