Formation of periodical metal oxide multilayer structures for the X-ray standing wave applications

TL;DR

This paper explores the design and fabrication of multilayer structures for X-ray standing wave applications, emphasizing the impact of structural defects and surface roughness on performance, with experimental validation using Ni/Al multilayers.

Contribution

It provides insights into the structural requirements for multilayers in XSW applications and demonstrates the viability of metal oxides as effective materials through experimental growth and surface analysis.

Findings

X-ray standing wave is robust against random multilayer imperfections.

Surface roughness significantly affects XSW experimental results.

Metal oxides can be effectively used as multilayer materials for XSW generators.

Abstract

Periodical multilayer (ML) structures can be used as generators of X-ray standing waves (XSW) for investigation of objects and processes on solid/liquid and solid/gas interfaces. In this paper, we investigate the specific requirements to the structural properties of the multilayer structures for XSW application. We consider the effect of typical defects in the ML structure on the X-ray standing wave formation and show that the X-ray standing wave is very robust against the random imperfection in the multilayer structure. In contrast, the roughness of the topmost layer will have a strong influence on the XSW experimental results, as the ML serves as a support for the investigated objects, so that the surface geometry gets directly translated into the objects. In the experimental part of this work, we have used the ion-beam deposition to grow Ni/Al metal- and metal oxide-based multilayers and investigate with AFM their surface quality. The presented results demonstrate that metal oxides can be successfully used as basic material for X-ray multilayer standing wave generators.