Strain hardening-softening oscillations induced by nanoindentation in bulk solids

TL;DR

This study introduces an empirical analysis method for nanoindentation data to reveal stress-strain oscillations and heterogeneities in bulk solids, showing oscillations linked to strain hardening-softening cycles at the microscale.

Contribution

It develops a novel technique to extract stress-strain field gradients and divergence from nanoindentation measurements, enhancing microstructural analysis of materials.

Findings

Oscillations in stress-strain field divergence are prominent at low indentation depths.

Amplitude of oscillations decays with depth following a power-law.

Oscillations correspond to strain hardening-softening cycles in subsurface layers.

Abstract

Nanoindentation is a widely used method for sensitive exploration of the mechanical properties of micromechanical systems. We derived an empirical analysis technique to extract stress-strain field gradient and divergence representations from nanoindentation measurements. With this approach local gradients and heterogeneities can be discovered to obtain more detail about the sample's microstructure, thus enhancing the analytic capacity of the nanoindentation technique. We analysed nanoindentation tests of bulk solid substrates, namely bearing and tooling steel, and fused silica. Oscillations of the stress-strain field gradient and divergence induced in the subsurface layer by the nanoindentation experiment were revealed. The oscillations were especially prominent in single measurements at low indentation depths (< 100 nm), whereas they were concealed in the averaged datasets. The amplitude of stress-strain field divergence oscillations decayed as a sublinear power-law when the indenter approached deeper atomic layers, with an exponent -0.9 for the steel and -0.8 for the fused silica. The oscillations were interpreted as alternating strain hardening-softening cycles induced in the subsurface layers under the indenter load. A selective assessment of elastic and plastic stress-strain field components indicated an elastic-plastic deformation process where the normal strain is transformed into the shear strain leading to a plastic deformation.