Carbon nanostructures obtained by underwater arc discharge of graphite electrodes: Synthesis and characterization

TL;DR

This paper explores the synthesis of various carbon nanostructures using underwater arc discharge of graphite electrodes, analyzing their morphology and structure with multiple microscopy and spectroscopy techniques.

Contribution

It demonstrates a method to produce diverse carbon nanostructures via underwater arc discharge and characterizes their features using advanced analytical tools.

Findings

Samples from water surface mainly contain onion-like particles.

Precipitate contains multiwalled nanotubes and other graphitic structures.

The method enables controlled synthesis of different nanostructures.

Abstract

In the present work, the application of the method of underwater arc discharge of graphite electrodes for obtaining several carbon nanostructures is described. The analysis of the obtained products by Transmission Electron Microscopy (TEM), Scanning Electron Microscopy (SEM), Raman spectroscopy, Atomic Force Microscopy (AFM) and X-Ray Diffraction (XRD) showed that the samples collected from the material floating on the water surface were composed mainly by polyhedral onion-like particles, while those taken from the precipitate were a mixture multiwalled nano-tubes, onion-like particles and other graphitic structures. The main features of the obtained nanostructures are discussed.