Corrections for the Geometric Distortion of the Tube Detectors on SANS Instruments at ORNL

TL;DR

This paper presents two methods for correcting geometric distortion in LPSD array detectors on SANS instruments, improving data accuracy for neutron scattering measurements.

Contribution

It introduces and compares two novel correction methods for geometric distortion in LPSD detectors, applicable to various SANS instruments.

Findings

Both methods produce consistent corrections with less than 0.05 deviation from isotropic scattering.

The correction techniques are effective up to a momentum transfer of 0.8 Å⁻¹.

Results are broadly applicable to LPSD-based SANS instruments worldwide.

Abstract

The small-angle neutron scattering instruments at the Oak Ridge National Laboratory High Flux Isotope Reactor recently upgraded the area detectors from the large, single volume crossed-wire detectors originally installed to staggered arrays of linear position-sensitive detectors, based on the design used on the EQ-SANS instrument at ORNL Spallation Neutron Source. The specific geometry of the LPSD array requires that approaches to data reduction traditionally employed be modified. Here, two methods for correcting the geometric distortion produced by the LPSD array are presented and compared. The first method applies a correction derived from a detector sensitivity measurement performed using the same configuration as the samples are measured. In the second method presented here, a solid angle correction derived for the LPSDs is applied to data collected in any instrument configuration during the data reduction process in conjunction with a detector sensitivity measurement collected at a sufficiently long camera length where the geometric distortions are negligible. Both methods produce consistent results and yield a maximum deviation of corrected data from isotropic scattering samples of less than 0.05 for momentum transfers up to a maximum of 0.8 A-1. The results are broadly applicable to any SANS instrument employing LPSD array detectors, which will be increasingly common as instruments having higher incident flux are constructed at various neutron scattering facilities around the world.