Polycrystal model of the mechanical behavior of a Mo-TiC30vol.% metal-ceramic composite using a 3D microstructure map obtained by a dual beam FIB-SEM

TL;DR

This study develops a 3D microstructure-based polycrystal model to predict the mechanical behavior of a Mo-TiC30vol.% composite across a wide temperature range, highlighting the importance of realistic microstructure representation.

Contribution

The paper introduces a novel 3D microstructure modeling approach using FIB-SEM data for accurate simulation of a Mo-TiC composite's mechanical behavior, including damage evolution.

Findings

Percolating TiC skeleton influences mechanical response.

Model captures temperature-dependent plasticity mechanisms.

Realistic microstructure essential for accurate predictions.

Abstract

The mechanical behavior of a Mo-TiC30 vol.% ceramic-metal composite was investigated over a large temperature range (25^{\circ}C to 700^{\circ}C). High-energy X-ray tomography was used to reveal the percolation of the hard titanium carbide phase through the composite. Using a polycrystal approach for a two-phase material, finite element simulations were performed on a real 3D aggregate of the material. The 3D microstructure, used as starting configuration for the predictions, was obtained by serial-sectioning in a dual beam Focused Ion Beam (FIB)-Scanning Electron Microscope (SEM) coupled to an Electron Back Scattering Diffraction system (3D EBSD, EBSD tomography). The 3D aggregate consists of a molybdenum matrix and a percolating TiC skeleton. As most BCC metals, the molybdenum matrix phase is characterized by a change in the plasticity mechanisms with temperature. We used a polycrystal model for the BCC material, which was extended to two phases (TiC and Mo). The model parameters of the matrix were determined from experiments on pure molydenum. For all temperatures investigated, the TiC particles were considered as brittle. Gradual damage of the TiC particles was treated, based on an accumulative failure law that is approximated by an evolution of the apparent particle elastic stiffness. The model enabled us to determine the evolution of the local mechanical fields with deformation and temperature. We showed that a 3D aggregate representing the actual microstructure of the composite is required to understand the local and global mechanical properties of the studied composite.