Sub micron-precision sample holder for accurate re-positioning of samples in Scanning Force Microscopy

TL;DR

This paper introduces two compact, high-precision sample holders for Scanning Force Microscopy that enable accurate re-positioning of samples within about 100 nanometers, facilitating ex-situ sample manipulation and repeated imaging of the same region.

Contribution

The authors present two novel, simple, and compact sample holders that improve sample re-positioning accuracy in SFM to within 100 nanometers, compatible with commercial systems.

Findings

Achieved re-positioning accuracy of approximately 100 nanometers.

Enables ex-situ manipulation and repeated imaging without optical aids.

Compatible with existing commercial SFM systems.

Abstract

Scanning Probe Microscopy allows for extreme resolution down to the atomic scale. Unfortunately, total scanning range is rather limited, therefore finding a specific position on the sample is tedious. This is an important limitation of many Scanning Probe Microscopes, in particular when the sample has to be removed for some kind of treatment and then re-allocated to characterize the same position where the previous experiment had been performed. In the present work we describe two simple and compact sub micron-precision sample holders that can be easily integrated in to a commercial Scanning Force Microscopy system. The design is based either on a traditional kinematic mounting or on self-adjustment of the sample holder and the upper piece of the piezoelectric scanner as the glue used to assemble the final setup solidifies. With these sample holders a specific sample position is automatically recovered to within about 100 nanometers, and thus well within the typical range of a piezoelectric scanner. Our experimental setup therefore allows ex-situ manipulation of the sample and SFM imaging of the same region without the aid of an optical microscope, positioning marks and tedious re-allocation.